u/ComradeDave123

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I am writing up a mock lab report for an experiment (I didn't do the experiment myself it was carried out by a member of staff) and I have been given the NMR data from the first step of the experiment and I need to analyse the data using MestRenova. The problem I'm running into is that I cannot tell at all what the multiplicity of the peaks are and I'm not sure how to proceed. I've compared the spectra I've been given to the literature and the one I have seems much more complex. I also had an issue working out where the solvent peak was but I concluded it was overlapping with some of the proton peaks but I'm not 100% sure if that's correct so conformation there would be very helpful too. I've attached images of the data I was given, with a zoomed focus on the peaks I'm struggling with, and the analysis I've done on it so far as well as the spectra from the paper I was comparing it too.

u/ComradeDave123 — 16 days ago